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A homemade immersed solvent microextraction (SME) device was successfully developed for the trace enrichment of phenols from aqueous samples. A microdrop of butyl acetate was suspended from the tip of a microsyringe needle, immersed in an aqueous spiked solution for a preset time. The microdrop was then retracted into the microsyringe and injected directly into a gas chromatography–mass spectrometry...