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CuO–Al 2 O 3 systems with different Cu/Al ratios were prepared by the amorphous citrate process, and their catalytic activities for the dehydrocoupling of methanol to methyl formate were examined. In the CuO–Al 2 O 3 systems, CuAl 2 O 4 samples calcined at temperatures below 1000°C were partially reduced during the reaction at 310°C and decreased the...