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An oxo-bridged dirhenium(III,III) complex of tris(2-pyridylmethyl)amine (tpa) and its one-electron oxidized (III,IV) species, [Re 2 (μ-O)Cl 2 (tpa) 2 ] 3+,4+ have been prepared. They are new members to a series of rhenium tpa complexes in various oxidation states. X-ray structural determination of the Re 2 (III,IV) complex revealed practically...