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We report that polycrystalline MOMONS (3-methoxy-4-methoxy-4'-nitrostilbene) shows a nonlinear optical (NLO) frequency doubling effect, and its d eff is 0.2-3 times that of d KDP and is dependent on the different particle sizes. MOMONS crystals have been grown from the melt by the Bridgman method but the crystals were not showing the NLO properties of the polycrystalline materials,...