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LiCo 1−x Mg x O 2 (x=0, 0.01, 0.03, and 0.05) was synthesized by a polymer-pyrolysis method. The effect of Mg doping on the structure and electrochemical properties of LiCoO 2 was investigated. XRD analysis showed that all the samples obtained had the well-ordered layer structure. SEM image showed that the powders consist of well-crystallized particles with hexagonal...