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We have designed new cleavable cross-linkers for biomolecules containing the 2,6-bis(oxazolinyl)pyridine (pybox) lanthanum complex. These species can effectively donate multiple charges to afford cross-linker ions for target biomolecules. The cross-linkers are cleaved easily by adding water. Moreover, we were able to detect chain structures of target molecules, including biomolecules and carbon clusters,...
An effective 15 N- and deuterium (D)-labeled 2,6-bis(oxazolin-2-yl)pyridine (pybox)–La complex based probe ionization method that produces a distinct isotopic shift was developed. The distinct isotopic shift was detected by using the newly synthesized 15 N-D-labeled pybox complexes. Moreover, O-[3-(tetramethylpybox)-propyl]-hydroxylamine (oxime–TMpybox) was prepared for attachment...
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