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The pure Ni and Ni-S ageing systems, thermally aged and also irradiated by 5 MeV electrons at 270 K with subsequent annealing, are studied by means of positron annihilation spectroscopy. The formation of ultrafine S-rich precipitates (clusters) is observed in Ni-S during thermal ageing at about 650 K. It is assumed that these clusters do not contain vacancy-type defects and they are coherent to the...