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The 1 : 1 type double salt of AgNO3 and NH4NO3 (NH4NO3 ⋅ AgNO3, compound 1) was prepared and its Raman spectrum was evaluated. IR and far‐IR spectra of compound 1 and its deuterated analog (ND4NO3 ⋅ AgNO3, compound 1‐D) were also studied. We identified two types of nitrate ions, one had a relatively strong, whereas the other is only weakly hydrogen bonded to the surrounding ammonium ions. The thermal...