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Gold nanoparticles were in situ synthesized via irradiation process, using PVA, (PVA:Cs), and (PVA:PAM) as host polymeric matrices. The effect of irradiation dose, polymer content, polymer combination AgNO3, chitosan, and poly acrylamide were studied. Gold nanoparticles (AuNPs) have spherical nanoparticles shape with different size ranging from 10−35 nm, which were characterized by ultraviolet‐visible...