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In this research, the kinetics and equilibrium of nickel(II) biosorption were studied in aqueous solutions using batch technique. The biosorption was carried on Ca‐alginate beads, on nonliving mycelium of Aspergillus awamori immobilized on Ca‐alginate, and on free fungal biomass. The biosorbents were characterized by FTIR and SEM analyses. The experimental data were analyzed in terms of pseudo‐first‐order,...