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An efficient synthetic method was developed for the preparation of 1‐octacosanol (C28‐alcohol) from commercially available lipid‐based intermediates namely sebacic acid (decanedioic acid) and stearyl alcohol. The key step in the synthesis is the preparation of tert‐butyl dimethyl octacos‐10‐enyloxy silane from 10‐tert‐butyl dimethyl silanyloxy decanal and octadecyl triphenylphosphonium bromide salt...