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Nanosized Pd17Se15 and PdP2 were synthesized at moderate temperature (using less toxic TOPO in case of PdP2) and explored for the first time to catalyze transfer hydrogenation (TH) of aldehydes / ketones using 2‐propanol as a source of hydrogen. The optimum catalyst loading was equivalent to 1.0 mol % of Pd. The round shaped Pd17Se15 NPs (15 to 30 nm), resulted on reacting (3‐(phenylseleno)propylamine)...