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An efficient and green method for synthesizing 3‐methyl‐4‐(hetero) arylmethylene isoxazole‐5(4H)‐ones was developed using a recyclable and environmental–friendly catalyst, Na2S2O3, and 16 target compounds were successfully synthesized under the obtained optimal reaction condition. Using rifampicin as a positive control, the antibacterial activity of all synthesized compounds was tested by micro dilution...