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The catalytic activity of CeO2 and palladium nanoparticles supported fly ash zeolite (CeO2/Pd@FAZ) for Csp2‐Csp2 bond formation was studied. CeO2/Pd@FAZ was characterized by FTIR, XRD, EDAX and TEM studies. In the Suzuki‐Miyauracross‐coupling reaction, biphenyl derivatives with excellent yields were obtained, and the reaction conditions were optimized. The catalytic activity was explored using a wide...