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A semi-organic nonlinear optical diguanidinum hydrogen phosphate monohydrate (G2HP) single crystal was synthesized by slow solvent evaporation technique. Single crystal XRD analysis was done on the grown semi-organic crystal G2HP. It reveals that the title compound has crystallized in a non-centrosymmetric tetragonal system with space group $${\text{P}}\bar{4}2_{1} {\text{c}}$$ P 4 ¯ 2...