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A Si–TiFeSi 2 composite was synthesized in large-scale using arc melting followed by rapid quenching. The composite showed that active Si nanocrystallites of approximately 50nm were embedded in an inactive TiFeSi 2 hard matrix. Crystalline Si reacted with Li to form the Li 21 Si 8 phase and transformed into amorphous Si when Li was extracted, while the TiFeSi 2...
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