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One new one-dimensional polymeric complex [Cd(C5H6N2)2(SeCN)2]n (1) has been synthesized and characterized by elemental analyses, spectroscopic studies and single crystal X-ray crystallography. Crystal structure shows the one-dimensional chain is propagated through doubly bridging selenocyanate and 4-aminopyridine acts as terminal ligand. The complex was characterized by fluorescence and NMR spectral...