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A series of iron/titanium oxide nanocrystalline particles with Fe/Ti molar ratios up to 0.15 were synthesized by a modified sol-gel technique using Ti(IV)-isopropoxide and anhydrous Fe(II)-acetate. The precursors were mixed and subsequently hydrolyzed with water molecules generated in situ by an esterification reaction between acetic acid and ethanol. As-synthesized samples were amorphous for XRD,...