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Pyridinecarboxamide binary phase diagrams have been established using differential scanning calorimetry, infrared spectroscopy and X-ray powder diffraction. Simulated diagrams obtained using with the Schröder-van Laar and Prigogine–Defay equations are in very good agreement with experimental data. The binary systems nicotinamide (Form I)–picolinamide (Form II) and isonicotinamide (Form II)—picolinamide...
Near-infrared (NIR) spectroscopy as a process monitoring and process supervision technique is reviewed in the context of biomanufacturing. An industrial pilot-plant mammalian cell cultivation process has been chosen to illustrate the use of on-line in-situ NIR monitoring by means of an immersion transflectance NIR probe. NIR calibration development must be performed carefully and should...
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