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Samples of lanthanum lithium titanate with the general formula La2/3 − xLi3xTiO3 with a different vacancy content, which is varied by varying the ratio of lanthanum to lithium, are investigated. Methods of synthesis, neutron diffraction data for the samples obtained, measurements of the lithium-ion conductivity of equilibrium and quenched samples, the results of nuclear magnetic resonance on 7Li...