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The Ca1−2xCe2xMo1−xGexO4 (0 ≤ × ≤ 0.2) micro/nanosized powders were prepared by aqueous nitrate-tartrate sol-gel synthesis. The obtained samples were characterized by XRD analysis, SEM microscopy, and IR spectroscopy. It was shown, that increase of cerium concentration in the series of compounds does not lead to obvious changes in their crystal structure, but changes of unit cell lattice parameters...