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A micellar polyoxometalate catalyst [C 16 H 33 N(CH 3 ) 3 ] 7 [PW 10 Ti 2 O 38 (O 2 ) 2 ] was prepared and used for catalytic wet air oxidation of thiocyanate (SCN − ). The 97.6% removal efficiency was obtained with oxygen and under room conditions. And the oxidation of SCN − was achieved completely leading...