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Remarkable differences have been observed between the host-guest interaction modes in two closely related crystalline inclusion compounds [1.MeOH (1:1) and 1.EtOH(1:1)] of the same carboxylic host (1). The minor modification of the guest structure crucially affected the hydrogen bonding recognition pattern between given complementary groups, which demonstrates the sensitive balance of intermolecular...
A convergent enantioselective total synthesis of the natural product (-)-balanol (1) is described. In addition to benzophenone fragment 8, key intermediates are chiral bicyclic aziridine 3 and the corresponding epoxide 4, both of which undergo highly regio- and stereoselective nucleophilic ring-opening reactions, allowing control of the two stereogenic centres of the target molecule. The structure...
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