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Reaction of Ag(BF 4 ) with [n-Bu 4 N][TCNQ] in CH 3 CN yields a new phase of Ag(TCNQ) referred to as phase I (1). A second polymorph of Ag(TCNQ), denoted phase II (2), which had earlier been prepared by electrocrystallization methods, can be accessed directly from silver powder and neutral TCNQ. The products were characterized by a combination of spectroscopic and physical...