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A series of quaternary Ni-Al-Me-C (Me=Ti, Nb or V) alloys and two Ni-Al-Nb alloys from various areas of the Ni-Al phase diagram were prepared by the mechanical alloying (MA) method starting from pure powder mixtures. X-ray diffraction and differential scanning calorimetry were used to investigate the powder alloys. It was found, that MA results in the formation of partially ordered metastable B2-type...