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Two new phosphate halides BaMnIII[PO4]FCl (1) and BaMnIII[PO4]F2 (2), have been synthesized under hydrothermal conditions. Structural characterizations show that both new compounds adopt layered structures but with different polyhedral linkages. Introduction of Cl into Compound (1) results in isolated hemimorphic [MnO4FCl] octahedra, different from the chain of [MnO4F2]/[MnO2F4] octahedra in Compound...