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Copolymers of aniline (ANI) and 2-methoxyaniline (MOA) in variable ratios, as well as the corresponding homopolymers, were electrosynthesized and characterized by elemental analysis, IR spectroscopy, and direct laser desorption ionization. The resulting copolymer composition obtained from the analysis was correlated with the feed composition through the Mayo–Lewis equation, confirming the higher reactivity...