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A nitrogen-sulfur Schiff base HL (1) derived from S-hexyldithiocarbazate and 4-methylbenzaldehyde has been reacted with different divalent metal ions in 2:1 molar ratio, producing neutral complexes (2–7) of general formula MIIL2 (where M=Ni, Cu, Zn, Cd, Pd and Pb). All compounds were characterized using established physico-chemical and spectroscopic methods. The single crystal structures of CuII and...
Divalent metal complexes of empirical formulation [ML2] (where M(II)=Ni, Cu, Zn, Cd and Pd; L=anionic form of the 2-thiophenecarboxaldehyde Schiff base of S-hexyldithiocarbazate) have been synthesized and characterized by physico-chemical techniques. Magnetic and spectroscopic data give support to a square-planar coordination geometry for these complexes with the exception of the ZnII and CdII species...
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