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The X-ray crystal structure analysis of [(L 2 )Rh(μ-κ 2 O,O'-HCO 2 ) 2 Rh(L' 2 )] 1a (L 2 = L' 2 =cod) is reported. Complex 1a reacts with CO to form 1c (L = L' = CO) via the intermediate 1b (L 2 = cod, L' = CO). 1a and 1c do not incorporate 13 CO 2 or D 2 in the formate moiety and are poor catalysts for...