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Benzothiazolium bromides (NSHC.HBr) (1a-j) with a variety of alkyl chain or benzyl substituents on N atom were prepared. The synthesis of ruthenium(II) (NSHC) complexes, (2a–j) could be achieved by in situ deprotonation of benzothiazolium salts with Ag2O and [RuCl2(p-cymene)]2. They were characterized by 1H, 13C, 19F NMR, IR spectroscopy and elemental analysis. The molecular structures of 2d, 2e and...