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A new process for electrolytic production of a perfluorinated compound, (CF 3 ) 3 N, using lanthanum nickel oxide-coated Ni sheet anode in the (CH 3 ) 4 NF·4.0HF melt at room temperature, was developed. Thin films of the lanthanum nickel oxides were prepared on Ni sheets by sol-gel coating method using polyvinlylpyrrolidone(PVP). The main components of the thin films...
A new process for electrolytic synthesis of a perfluorinated compound using mixed melts of (CH 3 ) 4 NF.4.0HF+xwt.% CsF.2.0HF as electrolytes and Ni sheet anode at room temperature was developed. The addition of CsF.2.0HF reduced the overvoltage of the Ni anode. The surface film on the anode formed in the presence of CsF.2.0HF consisted of inorganic compounds of NiF 2 , CsNi...
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