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A new environmental cell allowing for the independent synchronous collection of the near- and mid-infrared spectra (12,000–600cm −1 ) in the diffuse reflection and attenuated total reflection (ATR) modes, respectively, is reported. The cell is employed to study in real time the dehydration of the phyllosilicate mineral sepiolite, Mg 8 Si 12 O 30 (OH) 4 (OH ...