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The dolabellane‐type diterpene dictyoxetane represents a significant challenge to synthetic organic chemistry. Methodology directed towards the total synthesis of naturally occurring (+)‐dictyoxetane is reported. Catalytic asymmetric synthesis of the trans‐hydrindane ring system is achieved through chemoselective deoxygenation of the Hajos‐Parrish ketone. An alternative to the Garst‐Spencer furan...
Chemoenzymatic synthesis and modification of well-defined macrolactonic sophorolipid (SLML) analogues via a series of successive regioselective de-esterification/transesterification reactions is investigated. Of the lipases screened, Candida antartica lipase- B (Novozyme-435) successfully deacylated the C-6′ acetoxy group of natural and peracylated SLMLs. Subsequent transesterification with acylating...
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