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Electrochemical oxidation of cadmium in a solution of 4-methyl-6-trifluoromethylpyrimidine-2-thione (MeCF 3 -pymtH) in acetonitrile gave [Cd(MeCF 3 -pymt) 2 ], whose crystal structure has been determined by X-ray diffraction. The structure of the compound consists of polymeric chains containing octahedrally cis coordinated cadmium atoms (CdN 2 S 4 ), with each...
The electrochemical oxidation of anodic manganese in an acetonitrile solution of pyrimidine-2-thione (pymtH) or 4,6-dimethylpyrimidine-2-thione (4,6-Me 2 pymtH) and nitrogen donor bidentate ligands such as 1,10-phenanthroline (phen) or 2,2 -bipyridine (bipy), yielded mixed complexes [Mn(pymt) 2 phen], [Mn(4,6-Me 2 pymt) 2 phen] and [Mn(4,6-Me 2 pymt) 2...
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