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BaCe 0.9 Nd 0.1 O 3-δ was prepared through different routes: oxalate coprecipitation (OP), carbonate-oxide mixed by ball-milling (COB) and carbonate-oxide mixed by mortar/pestle (COM). The reaction process studied by DTA-TG and XRD showed that calcination of the precursor powders at T ≥ 1000°C could produce a single perovskite phase for all the...