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A response surface design of experiment (DOE) was developed to model crystallographic changes of UO2 and α-U3O8 after aging at elevated temperatures in controlled oxygen environments. Crystallographic changes to UO2 and α-U3O8 were quantified using powder X-ray diffractometry (p-XRD). In total, 108 samples were analyzed to build the DOE model on aging between 2 and 48 h, temperatures from 100 °C to...