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Stopped-flow measurements have been successfully combined with time-resolved UV/vis spectroscopy and global spectral analysis of superoxide decay for the comparative study of catalytic activity of putative manganese SOD (superoxide dismutase) mimetics known in the literature. The SOD activity of the studied complexes decreases in the following order: a) M40403>Mn(III)TM-4-PyP 5+ >Mn(II)pyane...