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In methanol, the reaction of Ti(O i Pr) 4 , N-(2-hydroxyphenyl)salicylideneimine (H 2 Sap) and 8-hydroxyquinoline (HQ) in stoichiometric ratio 1:1:x yielded Ti(Sap) 2 precipitate as initial product even when x was as high as 10. However, when the reaction mixture with x=2 was left standing for 12h or more, a small amount of red crystalline Ti(Sap)Q(OMe) was isolated...