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Reaction of i Pr 2 PCl with (Me 3 Si) 2 NH gives i Pr 2 PNH i PPr 2 (not isolated) which was oxidised with sulfur/selenium/oxygen to give i Pr 2 P(E)NHP(E') i Pr 2 (E, E'=Se; E=Se, E'=S; E=S, E'=O; E,E'=O). These neutral LH molecules readily undergo deprotonation/complexation to form simple ML 2 ...
Reaction of PtCl 2 (cod) with Pr i2 P(S)NHP(S)Pr i2 gives [M{N(Pr i2 PS) 2 } 2 ] (M = Pt1 , Pd 2). Repeated crystallization of the palladium complex from CH 2 Cl 2 resulted in the protonation of one ligand to give [Pd{HN(Pr i2 PS) 2 }]Cl. The X-ray structures of 1 and 2 reveal a dramatic change from...
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