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The 2,2,2-trichloroethoxycarbonyl (Troc) group was efficiently removed in high yields with (Bu 3 Sn) 2 in DMF under microwave heating. The present method was applied to deprotection of the Troc group on solid support.
Highly α-selective glucosylation was effected by virtue of the solvent effect of cyclopentyl methyl ether and the long-range assistance of bulky 6-O-protective groups. Higher α-selectivity was obtained by the use of this solvent in comparison to conventional diethyl ether. α-Selectivity was further improved with the influence of 6-O-substituents, such as TBDPS and phthaloyl groups, the latter being...
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