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BiSbO 4 powder was synthesized by a solid state reaction method. The sample was characterized by X-ray diffraction and UV–vis diffuse reflectance spectra. BiSbO 4 is an indirect gap material with the intrinsic band gap of 2.75eV. It possesses a fair activity for visible-light-driven photocatalysis. The results concerning methylene blue photodecomposition generally show that the catalytic...