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The thermal degradation of Nylon 6 has been studied over the temperature range 350–500°C by pyrolysis–gas chromatography. Samples in the microgram range were deposited as thin films on a pyrolysis filament with the capacity to reach the degradation temperature in ca. 20 ms, and under these conditions it was found that caprolactam monomer was produced almost exclusively. Kinetic measurements were made...