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The successful development of a laboratory scale integrated trial plant, a microplant, was demonstrated. The operation was evaluated using the etherification of 2-ethoxy-2-methylbutane as a demonstration case. The experimental results were validated against the literature data with good correlation thus proving that the microplant can be used efficiently for the scale-up of chemical industry processes...
An accurate control of reflux and reboil flow rates for small scale distillation unit has been evaluated. Its feasibility was studied with a distillation column with good results. The distillation column was planar in shape, and it was operated in a horizontal orientation. Porous, open-cell metal foam was used as the column packing. The distillation unit could be operated at extremely low mass fluxes...
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