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The potential of the 2-D INADEQUATE NMR experiment for identifying different 13 C⧹ 13 C connectivities and distinguishing between signals of compounds with very similar structures is demonstrated for two mixtures: quinoline and 3-acetyl pyridine, and n-propanol and 1,2-propanediol, and for the isomeric forms of the two disaccharides: cellobiose and maltose. The 1-D 13 C NMR...