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The syntheses of three ferrocenoyl peptides (Fc-GG-OEt (2), Fc-AA-OBzl (3), Fc-LF-OMe (4)) including their full spectroscopic characterization is reported. Titration of peptide solution with 3-aminopyrazole (APzl) in CDCl 3 was followed by 1 H-NMR spectroscopy and evaluated using Job's method and by non-linear regression. It was found that 4 showed the strongest interaction with APzl,...