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Four new Ag(I)–N‐heterocyclic carbene (NHC) complexes (5–8) bearing symmetrically substituted NHC ligands have been synthesized starting from the corresponding benzimidazolium bromide salts which are accessible in a single step from N‐substituted benzimidazoles (N‐alkyl and N‐aryl) and subsequently reacted with the basic metal source Ag2O in acetonitrile–methanol. These compounds were characterized...
Conventional bench top and solvothermal synthesis are determined to be reliable methods in the synthesis of coordination compounds containing the dicyanonitromethanide (dcnom) anion. From conventional bench top synthesis, [Ni(phen) 3 ](dcnom) 2 (1a), [Cu(phen) 3 ](dcnom) 2 (1b), [Cu(en) 3 ](dcnom) 2 (4), [Cu 3 (Hpz) 3 (H 2 O)(OH)(pz)...
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