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Phosphorus doped graphitic carbon nitride (g-C3N4) was easily synthesized using ammonium hexafluorophosphate (NH4PF6) as phosphorus source, and ammonium thiocyanate (NH4SCN) as g-C3N4 precursor, through a direct thermal co-polycondensation procedure. The obtained phosphorus doped g-C3N4 was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), high-resolution...
Ball-in-ball CuSCN hollow architecture is successfully synthesized by a facile one-pot aqueous solution method in the presence of poly(vinylpyrrolidone) at room temperature. The as-synthesized products are characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), high-resolution transmission electron microscopy (HRTEM), X-ray photoelectron spectroscopy (XPS), UV–vis...
In this paper, dynamic mechanical analysis (DMA), dielectric spectroscopy (DS) and positron annihilation lifetime spectroscopy (PALS) were used to study chlorinated butyl rubber (CIIR), in order to shed light on its unique relaxation behaviors. The dynamic mechanical loss tangent of CIIR reveals an asymmetrical broad structure with a maximum peak on the high-temperature side and a shoulder peak on...
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