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The photochemical disproportionation mechanism of [CpW(CO) 3 ] 2 in the presence of Lewis bases PR 3 was investigated on the nano- and microsecond time-scales with step-scan FTIR time-resolved infrared spectroscopy. Laser excitation (532nm) was used to homolytically cleave the W–W bond, forming the 17-electron radicals CpW(CO) 3 and initiating the reaction. With the...
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