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Hydrogen evolution from acidic aqueous solutions of TiIIIcitrate is strongly catalyzed by Co(dmgBF2)2. The reaction generates an intermediate with maximum absorbance at 770 nm. The slow disappearance of this intermediate takes place simultaneously with the generation of H2 in a process that was most efficient at pH 1.6 (turnover number 53). The loss of the catalytic activity is caused by the loss...
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