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Nanospheres of pyrochlore ammonium tungstate with an average diameter of 80nm are formed quantitatively via the one-step solvothermal reaction of ammonium metatungstate in the presence of an organic amine. The key solvothermal reaction parameters for pyrochlore formation are outlined. Morphology control is exerted over two length scales: the nanospheres are composed of nanorods with diameters around...
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